Winemaking (rec.crafts.winemaking) Discussion of the process, recipes, tips, techniques and general exchange of lore on the process, methods and history of wine making. Includes traditional grape wines, sparkling wines & champagnes.

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  #1 (permalink)   Report Post  
steve
 
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Default Filtering out ML bacteria

I have a BonVino Suprajet filter, and the finest filter pads I can get
locally are #3, which are described as 0.5 microns - sterile filtering. In
the interests of stabilizing a white wine I would prefer didn't go through
Malo - is this pad fine enough, or where can I get one fine enough? I have
consulted with a colleague who claims to use winery grade pads in his
Suprajet to filter out the wee beasties - but I didn't ask him for his
source.

Lysozome appears not to have done the trick - or wasn't done is sufficient
volume to slay them.

regards,
steve


  #2 (permalink)   Report Post  
Tom S
 
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Default Filtering out ML bacteria


"steve" > wrote in message
...
> I have a BonVino Suprajet filter, and the finest filter pads I can get
> locally are #3, which are described as 0.5 microns - sterile filtering. In
> the interests of stabilizing a white wine I would prefer didn't go through
> Malo - is this pad fine enough, or where can I get one fine enough? I have
> consulted with a colleague who claims to use winery grade pads in his
> Suprajet to filter out the wee beasties - but I didn't ask him for his
> source.


You'd need a 0.45 micron _absolute_ sterile membrane to filter out ML. A
0.5 micron nominal pad won't do it. Same goes if you are trying to remove
yeast from a sweet wine.

Tom S


  #3 (permalink)   Report Post  
LG1111
 
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Default Filtering out ML bacteria

>You'd need a 0.45 micron _absolute_ sterile membrane to filter out ML. A
>0.5 micron nominal pad won't do it. Same goes if you are trying to remove
>yeast from a sweet wine.
>
>Tom S


  #4 (permalink)   Report Post  
LG1111
 
Posts: n/a
Default Filtering out ML bacteria

>You'd need a 0.45 micron _absolute_ sterile membrane to filter out ML. A
>0.5 micron nominal pad won't do it. Same goes if you are trying to remove
>yeast from a sweet wine.
>
>Tom S
>

This whole business of filtering out bacteria just doesn't make any sense to
me. As a person who has to rely on sterile technique, I can say that there's
no half way point with sterility. Things are either sterile or they're growing
bugs, though possibly not in as high numbers. When you use a filter, there's
lots of leakage and dripping, so even if the filter was 0.45 microns, there
would still be contamination.

Add to that the fact that there has GOT to be a variation in the pore size.
Even if the average size is 0.45, then there have to be some pores that are
much larger.

I think filters do a great job in clarifying wine, but I've never had any luck
filtering out organisms.

Lee
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bob
 
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Default Filtering out ML bacteria

I guess this question is for Lum, will the set up he has documented in
his manual have the ability to sterile filter the wine with those $25
water filters?


Bob


"Tom S" > wrote in message .com>...
> "steve" > wrote in message
> ...
> > I have a BonVino Suprajet filter, and the finest filter pads I can get
> > locally are #3, which are described as 0.5 microns - sterile filtering. In
> > the interests of stabilizing a white wine I would prefer didn't go through
> > Malo - is this pad fine enough, or where can I get one fine enough? I have
> > consulted with a colleague who claims to use winery grade pads in his
> > Suprajet to filter out the wee beasties - but I didn't ask him for his
> > source.

>
> You'd need a 0.45 micron _absolute_ sterile membrane to filter out ML. A
> 0.5 micron nominal pad won't do it. Same goes if you are trying to remove
> yeast from a sweet wine.
>
> Tom S



  #6 (permalink)   Report Post  
William Frazier
 
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Default Filtering out ML bacteria

Lee - I used to deal with sterilization (pharmaceuticals - injectables,
preparation of sterile water for mfg. of liquid products, etc.) in my work.
We relied on filtration, albeit with 0.22 micron absolute filters, plus an
integrity check after filtration. IMO filtration can be used to remove
bacteria and yeast cells. Of course most home winemakers don't have the
ability to check filter integrity. And in my basement there is great
potential for contamination downstream from the filter. Still if you are
careful in your preparation, use 0.22 micron filters, sanitize the filter
tubing and receiving vessels you can knock the numbers of organisms down
significantly if not totally. I would much rather filter a sweetened wine
before bottling than just bottle and hope for the best.

Bill Frazier
Olathe, Kansas USA

"LG1111" > wrote in message
...
> This whole business of filtering out bacteria just doesn't make any sense

to
> me. As a person who has to rely on sterile technique, I can say that

there's
> no half way point with sterility. Things are either sterile or they're

growing
> bugs, though possibly not in as high numbers. When you use a filter,

there's
> lots of leakage and dripping, so even if the filter was 0.45 microns,

there
> would still be contamination.
>
> Add to that the fact that there has GOT to be a variation in the pore

size.
> Even if the average size is 0.45, then there have to be some pores that

are
> much larger.
>
> I think filters do a great job in clarifying wine, but I've never had any

luck
> filtering out organisms.
>
> Lee



  #7 (permalink)   Report Post  
Tom S
 
Posts: n/a
Default Filtering out ML bacteria


"LG1111" > wrote in message
...
> >You'd need a 0.45 micron _absolute_ sterile membrane to filter out ML. A
> >0.5 micron nominal pad won't do it. Same goes if you are trying to

remove
> >yeast from a sweet wine.
> >
> >Tom S
> >

> This whole business of filtering out bacteria just doesn't make any sense

to
> me. As a person who has to rely on sterile technique, I can say that

there's
> no half way point with sterility.


That's true - but sterile filtration is orders of magnitude better than any
alternative. IOW, it's pretty damn good.

Things are either sterile or they're growing
> bugs, though possibly not in as high numbers.


Exactly! Orders of magnitude lower.

When you use a filter, there's
> lots of leakage and dripping, so even if the filter was 0.45 microns,

there
> would still be contamination.


Are you assuming that because a filter is leaking that it has also to be
backstreaming? Probably not.

> Add to that the fact that there has GOT to be a variation in the pore

size.
> Even if the average size is 0.45, then there have to be some pores that

are
> much larger.


Nope. That's why it's called an _absolute_ filter. And let me tell you,
those suckers are _expen$ive_!

As far as determining whether the filter is capable of true sterile
filtration, it's necessary to run a bubble point check on it. IIRC, you
push water through the filter using gas (nitrogen), increasing the pressure
slowly until the gas pushes through the membrane and produces bubbles on the
other side. The pore size can be calculated from the pressure required to
do this, which is a function of pressure and surface tension of water.

> I think filters do a great job in clarifying wine, but I've never had any

luck
> filtering out organisms.


You've never used a sterile membrane cartridge filter. They do this quite
well. The one thing I don't like about them is that they have a plasticy
kind of smell that they impart to the first few gallons of wine - at least
when they are new. Run some hot water through first. That helps get rid of
it.

Tom S


  #8 (permalink)   Report Post  
Lum
 
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Default Filtering out ML bacteria


"bob" > wrote in message
om...
> I guess this question is for Lum, will the set up he has documented in
> his manual have the ability to sterile filter the wine with those $25
> water filters?
>
>
> Bob


Hi Bob, the answer is no. Those $25 filter housing do not provide an
adequate seal with the membrane filter cartridges.
lum


  #9 (permalink)   Report Post  
bob
 
Posts: n/a
Default Filtering out ML bacteria

Thanks Lum,

I was thinking about getting the Super Jet Buon Vino but noticed that
their "sterile" filter pads are .5 microns . I searched this newsgroup
and found another thread pertaining to this very subject. I guess .5
microns isn't "sterile" enough to inhibit MLF so I'm not sure what
good the Super Jet is over a plain $25 plastic cartridge filter. Do
you or anyone else out there have any suggestions , advice, experience
with a fairly inexpensive way of sterilizing 100 gallons of wine?
Should I just use sorbate instead? To explain the sitiuation exactly,
I have 100 gallons of eastern chardonnay that I'm about to add
bentonite to and cold stabilize. I'm looking to make the wine
semi-dry( more towards the semi than the dry ) and want to inhibite
MLF in the bottle. I am going to add sugar to the wine because it is
dry now. Should I just "rough" filter it and address the
re-fermentation and MLF in the bottle problem with sorbate and SO2?
Any input would be greatly appreciated.

Bob

"Lum" > wrote in message >...
> "bob" > wrote in message
> om...
> > I guess this question is for Lum, will the set up he has documented in
> > his manual have the ability to sterile filter the wine with those $25
> > water filters?
> >
> >
> > Bob

>
> Hi Bob, the answer is no. Those $25 filter housing do not provide an
> adequate seal with the membrane filter cartridges.
> lum

  #10 (permalink)   Report Post  
Lum
 
Posts: n/a
Default Filtering out ML bacteria


"bob" > wrote in message
om...
> Thanks Lum,
>
> I was thinking about getting the Super Jet Buon Vino but noticed that
> their "sterile" filter pads are .5 microns . I searched this newsgroup
> and found another thread pertaining to this very subject. I guess .5
> microns isn't "sterile" enough to inhibit MLF so I'm not sure what
> good the Super Jet is over a plain $25 plastic cartridge filter. Do
> you or anyone else out there have any suggestions , advice, experience
> with a fairly inexpensive way of sterilizing 100 gallons of wine?
> Should I just use sorbate instead? To explain the sitiuation exactly,
> I have 100 gallons of eastern chardonnay that I'm about to add
> bentonite to and cold stabilize. I'm looking to make the wine
> semi-dry( more towards the semi than the dry ) and want to inhibite
> MLF in the bottle. I am going to add sugar to the wine because it is
> dry now. Should I just "rough" filter it and address the
> re-fermentation and MLF in the bottle problem with sorbate and SO2?
> Any input would be greatly appreciated.
>
> Bob


Sterile bottling involves more than just putting wine through a tight
filter. Bottles, corks, corker, etc must all be sterile.

We use the following technique to make an off-dry wine at the winery every
year:
(1) Add frozen juice (or sugar) and potassium sorbate to the wine.
(2) Adjust the molecular SO2 to 0.8 milligrams per liter.
(3) Remove as much yeast as possible with a tight pad filtration.
(4) Observe the wine for several weeks to be sure it is stable before
bottling.

Good luck
Lum,
Del Mar, California, USA





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bob
 
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Default Filtering out ML bacteria

Thanks Lum. I assume a tight filter is .45 microns or less. Do you
have any recommendations for small scale wineries/large scale home
winemakers as far as a filtering system goes?? Any input would be
greatly appreciated.


Bob

"Lum" > wrote in message >...
> "bob" > wrote in message
> om...
> > Thanks Lum,
> >
> > I was thinking about getting the Super Jet Buon Vino but noticed that
> > their "sterile" filter pads are .5 microns . I searched this newsgroup
> > and found another thread pertaining to this very subject. I guess .5
> > microns isn't "sterile" enough to inhibit MLF so I'm not sure what
> > good the Super Jet is over a plain $25 plastic cartridge filter. Do
> > you or anyone else out there have any suggestions , advice, experience
> > with a fairly inexpensive way of sterilizing 100 gallons of wine?
> > Should I just use sorbate instead? To explain the sitiuation exactly,
> > I have 100 gallons of eastern chardonnay that I'm about to add
> > bentonite to and cold stabilize. I'm looking to make the wine
> > semi-dry( more towards the semi than the dry ) and want to inhibite
> > MLF in the bottle. I am going to add sugar to the wine because it is
> > dry now. Should I just "rough" filter it and address the
> > re-fermentation and MLF in the bottle problem with sorbate and SO2?
> > Any input would be greatly appreciated.
> >
> > Bob

>
> Sterile bottling involves more than just putting wine through a tight
> filter. Bottles, corks, corker, etc must all be sterile.
>
> We use the following technique to make an off-dry wine at the winery every
> year:
> (1) Add frozen juice (or sugar) and potassium sorbate to the wine.
> (2) Adjust the molecular SO2 to 0.8 milligrams per liter.
> (3) Remove as much yeast as possible with a tight pad filtration.
> (4) Observe the wine for several weeks to be sure it is stable before
> bottling.
>
> Good luck
> Lum,
> Del Mar, California, USA

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Lum
 
Posts: n/a
Default Filtering out ML bacteria


"bob" > wrote in message
om...
> Thanks Lum. I assume a tight filter is .45 microns or less. Do you
> have any recommendations for small scale wineries/large scale home
> winemakers as far as a filtering system goes?? Any input would be
> greatly appreciated.
>
>
> Bob


It depends on the amount of wine being made. For small amounts (less than
50 gallons) I would use a $25.00 plastic housing and a $8.00, 0.5 micron
(nominal) filter cartridge. That will remove most of the yeast and some of
the bacteria, and it will filter 25 to 50 gallons of clean wine.

For larger amounts, I use a 20 by 20 cm pad filter holding four to eight
pads. I buy 40 by 40 cm, one micron porosity pads and cut them in four
pieces with a box knife. That way, each 20 by 20 pad costs about $0.40 and
four pads will filter 50 to 60 gallons of clean wine. BUT, the filter
plates for a pad filter will cost about $150.

Lum
Del Mar, California, USA



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Tom S
 
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Default Filtering out ML bacteria


"bob" > wrote in message
om...
> I assume a tight filter is .45 microns or less.


That would be 0.45µ _absolute_ if your intention is to render the wine free
of yeast and bacteria.

Do you
> have any recommendations for small scale wineries/large scale home
> winemakers as far as a filtering system goes?? Any input would be
> greatly appreciated.


I recommend that you check out D.E.filtration, but something like a Buon
Vino could be really useful for a barrel or two. Media is cheaper with a
D.E. setup, but pads are not terribly expensive either.

If you're considering future expansion of your operations, a plate & frame
filter is the way to go. Remember this, though: To do _sterile_
filtrations you need to run the wine through a _membrane_ filter, rated at
0.45µ _absolute_.

There's a simple test you can perform on your filtration apparatus to be
sure that it is sterile-tight. It's called a "bubble point". Basically,
what you do is push water through the filter with gas - typically nitrogen -
and measure the filter medium's breakdown pressure (after all the water's
been pushed through), and gas bubbles start to pass through the membrane.
IIRC, it's over 30 PSI for a 0.45µ membrane. (Ask the mfgr. They would
have the data.) If the bubbles start to come sooner, the membrane's
ruptured or there's a leak somewhere. It's up to you to figure out which.
If the bubble point has been reached without "passing gas", or it just
_barely_started_ to gas, you're good to go.

Did I mention that filtration is a PIA?

Tom S


  #14 (permalink)   Report Post  
bob
 
Posts: n/a
Default Filtering out ML bacteria

Thanks Lum and Tom, I really apreciate the info. Lum, Where could I
find filter plates for a pad filter? I already have a pump. Could I
get just the filter setup or could I build it myself to save some $$$
???? As I understand what I read Tom I can get pad filters treated
with DE. Is that correct?


Bob

"Tom S" > wrote in message .com>...
> "bob" > wrote in message
> om...
> > I assume a tight filter is .45 microns or less.

>
> That would be 0.45µ _absolute_ if your intention is to render the wine free
> of yeast and bacteria.
>
> Do you
> > have any recommendations for small scale wineries/large scale home
> > winemakers as far as a filtering system goes?? Any input would be
> > greatly appreciated.

>
> I recommend that you check out D.E.filtration, but something like a Buon
> Vino could be really useful for a barrel or two. Media is cheaper with a
> D.E. setup, but pads are not terribly expensive either.
>
> If you're considering future expansion of your operations, a plate & frame
> filter is the way to go. Remember this, though: To do _sterile_
> filtrations you need to run the wine through a _membrane_ filter, rated at
> 0.45µ _absolute_.
>
> There's a simple test you can perform on your filtration apparatus to be
> sure that it is sterile-tight. It's called a "bubble point". Basically,
> what you do is push water through the filter with gas - typically nitrogen -
> and measure the filter medium's breakdown pressure (after all the water's
> been pushed through), and gas bubbles start to pass through the membrane.
> IIRC, it's over 30 PSI for a 0.45µ membrane. (Ask the mfgr. They would
> have the data.) If the bubbles start to come sooner, the membrane's
> ruptured or there's a leak somewhere. It's up to you to figure out which.
> If the bubble point has been reached without "passing gas", or it just
> _barely_started_ to gas, you're good to go.
>
> Did I mention that filtration is a PIA?
>
> Tom S

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Lum
 
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Default Filtering out ML bacteria


"bob" > wrote in message
m...
> Thanks Lum and Tom, I really apreciate the info. Lum, Where could I
> find filter plates for a pad filter? I already have a pump. Could I
> get just the filter setup or could I build it myself to save some $$$
> ???? As I understand what I read Tom I can get pad filters treated
> with DE. Is that correct?
>
>
> Bob


Bob, I have no recommendation at this time. I would have recommended Marcon
Filters several months ago, but Mr. Marcon passed away and the filter plates
are no longer available.

Lum
Del Mar, California, USA



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