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Trav77 10-01-2007 01:11 AM

Racking and Sulphite
 
I've got a batch of Carignane wine aging in the carboy right now and
have a question about how much sulphite to add at each racking. Here's
what I've done so far:

50 ppm sulphite at crush, 50 ppm sulphite at the first racking (after
ML fermentation was finished in November). My plan is to do a 2nd
racking, adding oak chips, then leave it till the Fall - do a 3rd
racking then bottle a week or so later.

Given the sulphite I've already added, how much should I add at the 2nd
and 3rd rackings? pH is 3.55-3.60.

Thanks!


pp 10-01-2007 07:48 PM

Racking and Sulphite
 
The better and safer way would be to measure the free SO2 before
racking and do the addition based on that. If you want to ballpark it,
then I'd suggest 20-40ppm at the 2nd racking, probably closer to the
end of the range to be safe. I'd definitely do the free SO2 check on
the next racking if you're planning to bottle right after, aiming for
30ppm or so at bottling.

Pp

On Jan 9, 5:11 pm, "Trav77" > wrote:
> I've got a batch of Carignane wine aging in the carboy right now and
> have a question about how much sulphite to add at each racking. Here's
> what I've done so far:
>
> 50 ppm sulphite at crush, 50 ppm sulphite at the first racking (after
> ML fermentation was finished in November). My plan is to do a 2nd
> racking, adding oak chips, then leave it till the Fall - do a 3rd
> racking then bottle a week or so later.
>
> Given the sulphite I've already added, how much should I add at the 2nd
> and 3rd rackings? pH is 3.55-3.60.
>
> Thanks!



Pino[_2_] 11-01-2007 10:39 AM

Racking and Sulphite
 
pp wrote:
> The better and safer way would be to measure the free SO2 before
> racking and do the addition based on that. If you want to ballpark it,
> then I'd suggest 20-40ppm at the 2nd racking, probably closer to the
> end of the range to be safe. I'd definitely do the free SO2 check on
> the next racking if you're planning to bottle right after, aiming for
> 30ppm or so at bottling.


How does one calculate how to add 20-40ppm of SO2?


guy 11-01-2007 04:53 PM

Racking and Sulphite
 

Pino wrote:
> How does one calculate how to add 20-40ppm of SO2?


Potassium metabisulphite salt contains 57% free SO2 (by
weight). For x liters, to get y ppm (parts per million) = y mg/l (y
l)/ (0.57) = grams of potassium metabisulphite salt.

For 23 liters, to get 40 ppm (parts per million) =
(40 mg/l x 23 l)/(0.57) = 0.99 grams of potassium
metabisulphite salt.
HTH,
Guy


pp 11-01-2007 06:09 PM

Racking and Sulphite
 


On Jan 11, 2:39 am, "Pino" > wrote:
> How does one calculate how to add 20-40ppm of SO2?


Guy's answer gives you the exact amount. If you don't have a precision
scale, a reasonable compromise is: 1/4 teaspoon of potassium meta gives
about 50ppm of free SO2 for 5 US gals, so dilute this in a known amount
of water - say 20-25 ml - and then calculate how much of the solution
you need for your volume.

Ex., to get 20ppm for 6 US gals: the whole amount of 20ml would give
(50ppm x 5 gals) / 6 glas ~ 42 ppm for the 6 gals, so to get 20ppm, use
(20ml x 20) / 42 ~ 10ml of the solution.

This is not as precise but good enough as long as the 1/4 tsp
measurement is reasonably correct - Iverson recommends getting the
spoon form a pharmacy instead of using the usual kitchen tool.

Pp


guy 11-01-2007 09:26 PM

Racking and Sulphite
 

pp wrote:
> On Jan 11, 2:39 am, "Pino" > wrote:
> > How does one calculate how to add 20-40ppm of SO2?

>
> Guy's answer gives you the exact amount.
> Pp


Wrong pp! I gave the right solution but the wrong answer.
For 23 liters, to get 40 ppm (parts per million) =
(40 mg/l x 23 l)/(0.57) = 1614 mg or 1,61 grams of potassium
metabisulphite salt.

Easier solution is 40g x 23 l /570 = 1,61 g

Guy


Joe Sallustio 11-01-2007 10:49 PM

Racking and Sulphite
 
Guy,
You sure you want to divide? I think you need to multiply: 40mg/l*23
L*.57 or around 1/2 g.
Joe

guy wrote:
> pp wrote:
> > On Jan 11, 2:39 am, "Pino" > wrote:
> > > How does one calculate how to add 20-40ppm of SO2?

> >
> > Guy's answer gives you the exact amount.
> > Pp

>
> Wrong pp! I gave the right solution but the wrong answer.
> For 23 liters, to get 40 ppm (parts per million) =
> (40 mg/l x 23 l)/(0.57) = 1614 mg or 1,61 grams of potassium
> metabisulphite salt.
>
> Easier solution is 40g x 23 l /570 = 1,61 g
>
> Guy



Paul E. Lehmann 11-01-2007 11:14 PM

Racking and Sulphite
 
Joe Sallustio wrote:

> Guy,
> You sure you want to divide? I think you need
> to multiply: 40mg/l*23 L*.57 or around 1/2 g.
> Joe
>
> guy wrote:
>> pp wrote:
>> > On Jan 11, 2:39 am, "Pino"
>> > > wrote:
>> > > How does one calculate how to add 20-40ppm
>> > > of SO2?
>> >
>> > Guy's answer gives you the exact amount.
>> > Pp

>>
>> Wrong pp! I gave the right solution but the
>> wrong answer. For 23 liters, to get 40 ppm
>> (parts per million) = (40 mg/l x 23 l)/(0.57) =
>> 1614 mg or 1,61 grams of potassium
>> metabisulphite salt.
>>
>> Easier solution is 40g x 23 l /570 = 1,61 g
>>
>> Guy


I will let Guy answer but I think he was / is
correct. Approximately half (0.57) will be free
the rest will be bound so if you multiply by any
number less than one you get a smaller number.
You need almost twice as much total to get
approx. half of it as free. Multiplying will give
you only about 1/4 of what you need. I have
always been mathematically challenged - Ray
Calvert - where are you, math tutor. Are all
those beers we consumed tutoring me 35 years ago
for naught?

Joe Sallustio 12-01-2007 11:57 AM

Racking and Sulphite
 

> I will let Guy answer but I think he was / is
> correct. Approximately half (0.57) will be free
> the rest will be bound so if you multiply by any
> number less than one you get a smaller number.


I'm an idiot, you are right. No idea what I was thinking there. Guy
had it right. Sounds like Ray has to keep an eye on two of us now.

Joe


guy 12-01-2007 03:34 PM

Racking and Sulphite
 

Joe Sallustio wrote:
> I'm an idiot, you are right. No idea what I was thinking there. Guy
> had it right.>
> Joe


I don't blame you Joe, that / after the 40mg is confusing. Besides, I
made a mistake in my first post so....

Cheers,
Guy



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