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Winemaking (rec.crafts.winemaking) Discussion of the process, recipes, tips, techniques and general exchange of lore on the process, methods and history of wine making. Includes traditional grape wines, sparkling wines & champagnes.

Reducing acid - one year old wine



 
 
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  #1 (permalink)  
Old 16-08-2005, 03:23 AM
Fishhead
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Default Reducing acid - one year old wine

I have some merlot and cabernet that I made last year.

They both have a bit of excessive acid taste in them.

I tried the following reductions... and it has gone down but not enough.

Malo fermentation
Cold aging at 30°F (3 months)

What else can I do now?

Will finning help?
Age help?
chemical??

I blended 5gals of merlot with 3.5gals of cabernet.
This is the best of both of them... but still too much.

The PH is 3.85
I didn't read the acid, cause I am not too good at it.
  #2 (permalink)  
Old 16-08-2005, 04:40 AM
mnhudson@gmail.com
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Fishhead -
Fining generally doesn't alter the acidity. There are some
chemicals you can use (usually potassium or calcium carbonate are
recommended) but they do also alter the taste of the wine. If your pH
reading is accurate, your wine is already rather low in acid (high pH),
so I'd be reluctant to do anything to treat the wine further. Aging
alone shouldn't alter the acidity, but perhaps what you are
interpreting as acidity is something else. Tannins and/or alcohol
level also can produce a bit of a "sharp" taste that may come across to
some as too much acid. Some fining agents can reduce the tannins. Or
you could just let it age; this tends to soften the "sharpness" over
time. The other thing that tends to counteract the impression of
acidity is sweetness (sugar), but for these types of wine, you probably
don't want to sweeten them.

I'd recommend testing the acidity (even if you're not expert at
it) and re-checking the pH before you do anything further. If you made
these from grapes (not kits), they may just take a year to two to
really settle down. Patience is one of a winemaker's most essential
tools (not that it's easy to come by . . .)

Doug

  #3 (permalink)  
Old 16-08-2005, 05:01 AM
Fishhead
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Default

I calibrated my PH meter and re-checked everything.
I let a glass warm up some, and I think you might be correct.. maybe it
is something besides acid.
The cabernet was a bit high on the brix.
My vino-meter says close to 15%
The merlot was normal brix

I lost my acid test kit instructions, I forgot how to determine the
acid.. I thought it was the syringe * .25
I measured the color change at pH 8

Cab/merlot blend
pH is 3.85
2.2 * .25 = .55 TA
2.1 * .25 = .525 TA


I also checked a blueberry wine that I have been drinking. Which I think
is a bit tart

pH is 3.75
2.5 * .25 = .625 TA
2.4 * .25 = .600 TA


Maybe it is just age... I am in no hurry, just want to do it correct.
( I have plenty of beer to drink !)
  #4 (permalink)  
Old 16-08-2005, 05:06 AM
Fishhead
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Default

Could this also be excessive SO2?

I have been adding 1 tablet per gallon whenever I rack...
which is 5 times now.



Fishhead wrote:
I calibrated my PH meter and re-checked everything.
I let a glass warm up some, and I think you might be correct.. maybe it
is something besides acid.
The cabernet was a bit high on the brix.
My vino-meter says close to 15%
The merlot was normal brix

I lost my acid test kit instructions, I forgot how to determine the
acid.. I thought it was the syringe * .25
I measured the color change at pH 8

Cab/merlot blend
pH is 3.85
2.2 * .25 = .55 TA
2.1 * .25 = .525 TA


I also checked a blueberry wine that I have been drinking. Which I think
is a bit tart

pH is 3.75
2.5 * .25 = .625 TA
2.4 * .25 = .600 TA


Maybe it is just age... I am in no hurry, just want to do it correct.
( I have plenty of beer to drink !)

  #5 (permalink)  
Old 16-08-2005, 07:22 PM
Ray Calvert
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Default

You do have a problem. You have more acid taste than you like but your pH
is already higher than it should be. (Remember, high pH indicates low acid)
With that high of a pH you are probably going to have trouble aging this
wine very long. Normally you want a pH of below 3.50 for aging. Whether
you adjust the acid further or not, you want to be sure that you use
adequate sulfite and even then this may be a wine you want to drink young.

I hate it when wines come out with high acid AND high pH. Very difficult to
adjust properly.

Ray

"Fishhead" wrote in message
...
I have some merlot and cabernet that I made last year.

They both have a bit of excessive acid taste in them.

I tried the following reductions... and it has gone down but not enough.

Malo fermentation
Cold aging at 30°F (3 months)

What else can I do now?

Will finning help?
Age help?
chemical??

I blended 5gals of merlot with 3.5gals of cabernet.
This is the best of both of them... but still too much.

The PH is 3.85
I didn't read the acid, cause I am not too good at it.



  #6 (permalink)  
Old 16-08-2005, 08:41 PM
hombrewdude
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Default

So what are some suggestions for correcting it?

  #7 (permalink)  
Old 17-08-2005, 05:08 PM
Ray Calvert
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Default


"hombrewdude" wrote in message
ups.com...
So what are some suggestions for correcting it?


Good question! I have never found a reliable way. My suspicion is that
there is too much of the wrong type of acid. Maybe Lum has a suggestion.
This is more up his alley.

Ray


  #8 (permalink)  
Old 17-08-2005, 06:35 PM
pp
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Posts: n/a
Default


Ray Calvert wrote:
"hombrewdude" wrote in message
ups.com...
So what are some suggestions for correcting it?


Good question! I have never found a reliable way. My suspicion is that
there is too much of the wrong type of acid. Maybe Lum has a suggestion.
This is more up his alley.

Ray


The usual approach is to use tartaric to bring the pH down to about 3.6
and then cold stabilize the hell out of it. I have a Syrah from last
year that's at 3.9 and TA about 6.5, so the acidity is actually where I
want it. I took a sample bottle and added about 2g/L tartaric to bring
the pH down to 3.6, then froze it in the freezer for a week. When I
defrosted it and tested, the pH went down to 3.5 and the TA was exactly
the same as before - 6.5. So this test indicates that treating this
particular wine in this way should fix the pH problem. I would
definitely recommend a test though before comitting the whole batch, I
hate it when the reds end up too acidic.

Also, back to the sulfite - there is a chance there is too much in the
wine, so measure it too. If excessive, sulfite can give harshness to
the taste in the back of your throat, similar to acid.

Pp

  #9 (permalink)  
Old 18-08-2005, 12:48 AM
Fishhead
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Posts: n/a
Default

I can rack a gallon off and try this process

Is there a standard way to determine how much tartric to add to adjust?

What is the acid level I am shooting for in my merlot/cab blend?


pp wrote:
Ray Calvert wrote:

"hombrewdude" wrote in message
roups.com...

So what are some suggestions for correcting it?


Good question! I have never found a reliable way. My suspicion is that
there is too much of the wrong type of acid. Maybe Lum has a suggestion.
This is more up his alley.

Ray



The usual approach is to use tartaric to bring the pH down to about 3.6
and then cold stabilize the hell out of it. I have a Syrah from last
year that's at 3.9 and TA about 6.5, so the acidity is actually where I
want it. I took a sample bottle and added about 2g/L tartaric to bring
the pH down to 3.6, then froze it in the freezer for a week. When I
defrosted it and tested, the pH went down to 3.5 and the TA was exactly
the same as before - 6.5. So this test indicates that treating this
particular wine in this way should fix the pH problem. I would
definitely recommend a test though before comitting the whole batch, I
hate it when the reds end up too acidic.

Also, back to the sulfite - there is a chance there is too much in the
wine, so measure it too. If excessive, sulfite can give harshness to
the taste in the back of your throat, similar to acid.

Pp

  #10 (permalink)  
Old 18-08-2005, 01:55 AM
pp
Usenet poster
 
Posts: n/a
Default


Fishhead wrote:
I can rack a gallon off and try this process

Is there a standard way to determine how much tartric to add to adjust?


Not really. The common method is to make up a strong solution of
tartaric acid in water and then add a small measured amount (pipette or
syringe) into a sample of wine, say 1 litre. Then measure the pH and
repeat until the level gets to where you want it, say around 3.6-3.65.
Then from the amount of solution and size of the sample you can
calculate how much acid you've added in terms of g/L and from that you
can easily get the total amount for the whole batch.

Do the full test (including stabilization) for the sample and then
adjust based on the results. For example, in my case I've added 2g/L of
acid and the pH went lower in the end then I wanted, so I'd probably
add only about 1.5g/L to the full batch.

Also, I'm not sure how instant the pH change is after addition and
mixing, so it's probably better to remeasure the pH on the test sample
next day to get better data.

What is the acid level I am shooting for in my merlot/cab blend?


I would go by taste at this stage, numbers can be misleading. And you
won't know where the TA will end in the end because it will be pretty
high before cold stabilization and that process is pretty
unpredictable.

Also, I haven't decided myself if I'm doing the adjustment on the whole
batch because I can't get reliably get the wine to the 25F or so needed
for a thorough cold stabilization. My current thinking is I'll do 3
gallons in the interest of "research" and leave the rest (6 gallons)
alone for now.

Pp


pp wrote:
Ray Calvert wrote:

"hombrewdude" wrote in message
roups.com...

So what are some suggestions for correcting it?


Good question! I have never found a reliable way. My suspicion is that
there is too much of the wrong type of acid. Maybe Lum has a suggestion.
This is more up his alley.

Ray



The usual approach is to use tartaric to bring the pH down to about 3.6
and then cold stabilize the hell out of it. I have a Syrah from last
year that's at 3.9 and TA about 6.5, so the acidity is actually where I
want it. I took a sample bottle and added about 2g/L tartaric to bring
the pH down to 3.6, then froze it in the freezer for a week. When I
defrosted it and tested, the pH went down to 3.5 and the TA was exactly
the same as before - 6.5. So this test indicates that treating this
particular wine in this way should fix the pH problem. I would
definitely recommend a test though before comitting the whole batch, I
hate it when the reds end up too acidic.

Also, back to the sulfite - there is a chance there is too much in the
wine, so measure it too. If excessive, sulfite can give harshness to
the taste in the back of your throat, similar to acid.

Pp


  #11 (permalink)  
Old 21-08-2005, 12:15 PM
Joe Sallustio
Usenet poster
 
Posts: n/a
Default

That's an incredible amount of SO2, it's probably the issue. You have
added 5 times too much several times too many as I see it.

It's my understanding that 1 tablet per gallon equals around 100 PPM, I
ony add 20 PPM per rack and rack 3 times or less as a rule.

You can get titrettes to measure this, other ways like vacuum
aspiration are better but pretty costly. Just use the color of the
foam in the titrettes as an indication of change (end point).

If your acid test results are correct it's not that high, contact the
people you bought it from to determine if your process is correct.

High pH is an issue, but 3.85 is actually not out of the question.
Technically it's too high but I have had them last 5 years. If
anything they age quickly.

If it's too much sulfite, I would see how much it is and go from there.
I would calculate this as about 400 PPM if you let things splash when
you rack and that is 6 to 8 times too much. Blending with this years
wine may be the best option if that is the case.

Joe

  #12 (permalink)  
Old 21-08-2005, 09:55 PM
Paul E. Lehmann
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Posts: n/a
Default

Fishhead wrote:

Could this also be excessive SO2?

I have been adding 1 tablet per gallon whenever I rack...
which is 5 times now.


You can send a sample to Vinquiry and they will do an AO Free SO2 test for
$12.00 If you have a fair amount of wine and do not have AO test equipment
of your own you may wish to consider this. AO is suppose to be superior to
Ripper method for free SO2 determinations. Vinquiry will send you sample
bottles free of charge.

http://www.vinquiry.com/
  #13 (permalink)  
Old 22-08-2005, 05:15 AM
Fishhead
Usenet poster
 
Posts: n/a
Default

Paul E. Lehmann wrote:
Fishhead wrote:


Could this also be excessive SO2?

I have been adding 1 tablet per gallon whenever I rack...
which is 5 times now.



You can send a sample to Vinquiry and they will do an AO Free SO2 test for
$12.00 If you have a fair amount of wine and do not have AO test equipment
of your own you may wish to consider this. AO is suppose to be superior to
Ripper method for free SO2 determinations. Vinquiry will send you sample
bottles free of charge.

http://www.vinquiry.com/



Thanks
I only have a few 5 gal batches.
I am going to try to test this myself
  #14 (permalink)  
Old 22-08-2005, 08:18 PM
pp
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Posts: n/a
Default


Joe Sallustio wrote:
That's an incredible amount of SO2, it's probably the issue. You have
added 5 times too much several times too many as I see it.

It's my understanding that 1 tablet per gallon equals around 100 PPM, I
ony add 20 PPM per rack and rack 3 times or less as a rule.

You can get titrettes to measure this, other ways like vacuum
aspiration are better but pretty costly. Just use the color of the
foam in the titrettes as an indication of change (end point).

If your acid test results are correct it's not that high, contact the
people you bought it from to determine if your process is correct.

High pH is an issue, but 3.85 is actually not out of the question.
Technically it's too high but I have had them last 5 years. If
anything they age quickly.

If it's too much sulfite, I would see how much it is and go from there.
I would calculate this as about 400 PPM if you let things splash when
you rack and that is 6 to 8 times too much. Blending with this years
wine may be the best option if that is the case.

Joe


According to Ben's SO2 article, it's a bit lower - 67ppm for potassium
based tablets or 78ppm for sodium. But it's still way too much. At that
level, it should be plainly noticeable by smelling alone, even without
titrets.

Also, titrets are good only if the level is 100ppm, otherwise the
measurement is off the scale. If that happens, you can always dilute
the sample to a 1:1 or 1:2 ratio with distilled water and then measure
that.

Pp

 




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